C₁₆H₂₄O₃

Base Information

Chemical Name:C₁₆H₂₄O₃
CAS No.:1312136-36-9
Molecular Formula:C₁₆H₂₄O₃
Molecular Weight:264.365
Hs Code.:

C<sub>16</sub>H<sub>24</sub>O<sub>3</sub>

Synonyms:C₁₆H₂₄O₃

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Chemical Property of C₁₆H₂₄O₃

Chemical Property:

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Technology Process of C₁₆H₂₄O₃

There total 6 articles about C₁₆H₂₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 155887-05-1
(2R,4R)-4,5-(isopropylidenedioxy)-2-methylpentan-1-ol

: 1312136-36-9
C₁₆H₂₄O₃

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.3390/molecules16075422

Reference yield:

: 1312136-34-7
(R)-4-benzyl-3-(3-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-propanoyl)oxazolidin-2-one

: 1312136-36-9
C₁₆H₂₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -40 °C / Inert atmosphere

1.2: 4 h / -20 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran; methanol; water / 2.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With lithium borohydride; tetra-(n-butyl)ammonium iodide; sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 1.1: Evans asymmetric alkylation;
DOI:10.3390/molecules16075422

Reference yield:

: (R)-3-(2,2-dimethyl-1,3-dioxolan-4-yl)-2-propenoic acid methyl ester

: 1312136-36-9
C₁₆H₂₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / ethanol / 20 °C

2.1: lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C / Inert atmosphere

2.2: pH 4 / Inert atmosphere

3.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -40 °C / Inert atmosphere

4.2: 4 h / -20 °C / Inert atmosphere

5.1: lithium borohydride / tetrahydrofuran; methanol; water / 2.5 h / 0 - 20 °C / Inert atmosphere

5.2: 0 °C / Inert atmosphere

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With lithium borohydride; hydrogen; pivaloyl chloride; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; 4.1: Evans asymmetric alkylation;
DOI:10.3390/molecules16075422