C₁₄H₁₃ClN₄O

Base Information

Chemical Name:C₁₄H₁₃ClN₄O
CAS No.:1466565-99-0
Molecular Formula:C₁₄H₁₃ClN₄O
Molecular Weight:288.736
Hs Code.:

C<sub>14</sub>H<sub>13</sub>ClN<sub>4</sub>O

Synonyms:C₁₄H₁₃ClN₄O

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Chemical Property of C₁₄H₁₃ClN₄O

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Technology Process of C₁₄H₁₃ClN₄O

There total 8 articles about C₁₄H₁₃ClN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1466565-98-9
C₁₉H₂₁ClN₄O₃

: 1466565-99-0
C₁₄H₁₃ClN₄O

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 872-32-2
2-methyl-1H-pyrroline

: 1466565-99-0
C₁₄H₁₃ClN₄O

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-chloro-succinimide / tetrahydrofuran / 0.58 h / 55 °C

2.1: methanol / 2.5 h / 0 - 20 °C

3.1: lithium hydroxide / tetrahydrofuran; methanol / 1.5 h / 60 °C

4.1: thionyl chloride / 0.83 h / 75 °C / Inert atmosphere

4.2: 2 h / 0 - 60 °C / Inert atmosphere

5.1: sodium hydroxide; ammonium hydroxide; sodium hypochlorite; ammonium chloride / water; ethyl acetate; tert-butyl methyl ether / 2.5 h / 0 - 20 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 65 h / 20 °C

7.1: triphenylphosphine; iodine; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

8.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

With ammonium hydroxide; sodium hypochlorite; N-chloro-succinimide; thionyl chloride; iodine; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; tert-butyl methyl ether; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1466565-96-7
3-chloro-N-phenyl-1H-pyrrole-2-carboxamide

: 1466565-99-0
C₁₄H₁₃ClN₄O

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; ammonium hydroxide; sodium hypochlorite; ammonium chloride / water; ethyl acetate; tert-butyl methyl ether / 2.5 h / 0 - 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 65 h / 20 °C

3: triphenylphosphine; iodine; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

4: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

With ammonium hydroxide; sodium hypochlorite; iodine; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In dichloromethane; tert-butyl methyl ether; water; ethyl acetate; N,N-dimethyl-formamide;