(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

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Chemical Name:(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol
CAS No.:1270018-20-6
Molecular Formula:C₂₁H₂₂ClNO₆S
Molecular Weight:451.928
Hs Code.:

Synonyms:(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

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Chemical Property of (2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

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Technology Process of (2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

There total 3 articles about (2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1270018-18-2
((2R,3S,4R,5R,6S)-6-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-3,4,5-trihydroxy-tetrahydro-2H-pyran-2-yl)methyl 4-methylbenzenesulfonate

: 124-41-4
sodium methylate

: 1270018-20-6
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: In methanol; at 20 ℃; for 15h; Inert atmosphere;

Reference yield: 36.0%

: C₂₇H₂₆ClNO₇S₂

: 124-41-4
sodium methylate

: 1270018-20-6
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: In methanol; at 20 ℃; for 15h;
DOI:10.1016/j.bmcl.2010.11.115

Reference yield:

: 1260242-23-6
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

: 1270018-20-6
(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(furan-2-yl)thiazol-2-yl)methyl)phenyl)-6-(methoxymethyl)-tetrahydro-2H-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / 15 h / 20 °C

2: methanol / 15 h / 20 °C

With 2,6-dimethylpyridine; In methanol;
DOI:10.1016/j.bmcl.2010.11.115