C₄₂H₄₀BrCl₃N₂O₁₁S

Base Information

Chemical Name:C₄₂H₄₀BrCl₃N₂O₁₁S
CAS No.:1234550-88-9
Molecular Formula:C₄₂H₄₀BrCl₃N₂O₁₁S
Molecular Weight:967.115
Hs Code.:

C<sub>42</sub>H<sub>40</sub>BrCl<sub>3</sub>N<sub>2</sub>O<sub>11</sub>S

Synonyms:C₄₂H₄₀BrCl₃N₂O₁₁S

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Chemical Property of C₄₂H₄₀BrCl₃N₂O₁₁S

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Technology Process of C₄₂H₄₀BrCl₃N₂O₁₁S

There total 22 articles about C₄₂H₄₀BrCl₃N₂O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1234550-72-1
C₃₅H₃₄BrCl₃N₂O₁₁S

: 100-39-0
benzyl bromide

: 1234550-88-9
C₄₂H₄₀BrCl₃N₂O₁₁S

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo100788j

Reference yield:

: 1150635-60-1
C₂₂H₂₅NO₇

: 1234550-88-9
C₄₂H₄₀BrCl₃N₂O₁₁S

Guidance literature:: Multi-step reaction with 14 steps

1.1: methanol; potassium carbonate / 1 h / 0 °C / Inert atmosphere

1.2: 0 °C / pH 3

2.1: 10% palladium on activated carbon; hydrogen / methanol / 10 h / 20 °C / 760.05 Torr

3.1: N-Bromosuccinimide / acetonitrile / 1 h / 0 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

5.1: methanol; acetyl chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

6.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

6.2: 20 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: sodium hydrogencarbonate / dichloromethane; water / 2 h / 0 °C

8.1: tin(II) bromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

9.1: lithium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

9.2: 0 °C

10.1: (triphenylphosphine)gold(I) chloride; silver(I) triflimide / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

11.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

12.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

13.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

14.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With methanol; N-Bromosuccinimide; (triphenylphosphine)gold(I) chloride; lithium hydroxide monohydrate; 10% palladium on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; phenyltrimethylammonium tribromide; tin(II) bromide; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; potassium iodide; lithium hydroxide; silver(I) triflimide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 13.1: Friedel Crafts alkylation;
DOI:10.1021/jo100788j

Reference yield:

: 1177255-35-4
(S)-methyl 3-(2-bromo-5-hydroxy-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoate

: 1234550-88-9
C₄₂H₄₀BrCl₃N₂O₁₁S

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: methanol; acetyl chloride / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 20 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: sodium hydrogencarbonate / dichloromethane; water / 2 h / 0 °C

5.1: tin(II) bromide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

6.1: lithium hydroxide / tetrahydrofuran; methanol; water / 0 - 20 °C

6.2: 0 °C

7.1: (triphenylphosphine)gold(I) chloride; silver(I) triflimide / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

8.1: dichloromethane / 22 h / 20 °C / Inert atmosphere

9.1: magnesium sulfate; toluene-4-sulfonic acid / toluene / 12 h / 90 °C / Inert atmosphere

10.1: phenyltrimethylammonium tribromide / acetonitrile / 20 - 60 °C / Inert atmosphere; Molecular sieve

11.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With methanol; (triphenylphosphine)gold(I) chloride; lithium hydroxide monohydrate; tetra-(n-butyl)ammonium iodide; phenyltrimethylammonium tribromide; tin(II) bromide; sodium hydrogencarbonate; magnesium sulfate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; potassium iodide; lithium hydroxide; silver(I) triflimide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 10.1: Friedel Crafts alkylation;
DOI:10.1021/jo100788j