(E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

Base Information

Chemical Name:(E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine
CAS No.:1604832-28-1
Molecular Formula:C₁₈H₂₇NO₄
Molecular Weight:321.417
Hs Code.:

Synonyms:(E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

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Chemical Property of (E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

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Technology Process of (E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

There total 3 articles about (E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 92847-88-6
cyclopropyl(3,4-dimethoxyphenyl)methanone

: 645-36-3
2,2-diethoxy-ethanamine

: 1604832-28-1
(E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

Guidance literature:: In toluene; at 170 ℃; for 4h; Dean-Stark;

Reference yield: 94.0%

: 1604832-28-1
(E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

Guidance literature:: In toluene; at 150 ℃; for 4h; Dean-Stark;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 1604832-28-1
(E)-N-(cyclopropyl(3,4-dimethoxyphenyl)methylene)-2,2-diethoxyethanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / dichloromethane / 0.08 h / -4 °C / Inert atmosphere

1.2: 1.25 h / -4 - 0 °C / Inert atmosphere

2.1: toluene / 4 h / 170 °C / Dean-Stark

With aluminum (III) chloride; In dichloromethane; toluene; 1.1: |Friedel-Crafts Acylation / 1.2: |Friedel-Crafts Acylation;