ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate

Base Information

Chemical Name:ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate
CAS No.:931399-63-2
Molecular Formula:C₂₁H₂₁NO₆
Molecular Weight:383.401
Hs Code.:

Synonyms:ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate

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Chemical Property of ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate

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Technology Process of ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate

There total 1 articles about ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 100-39-0
benzyl bromide

: 81595-17-7
5,6-dimethoxy-1H-benzo[d][1,3]oxazine-2,4-dione

: 105-53-3
diethyl malonate

: 931399-63-2
ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate

Guidance literature:: benzyl bromide; 5,6-dimethoxy-1H-benzo[d][1,3]oxazine-2,4-dione; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

diethyl malonate; In N,N-dimethyl-formamide; at 150 ℃; for 0.333333h; Microwave;

Reference yield: 30.0%

: 931399-63-2
ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate

: 6000-44-8
sodium glycinate

: N-{[4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinyl]carbonyl}glycine

Guidance literature:: ethyl 4-hydroxy-5,6-bis(methyloxy)-2-oxo-1-(phenylmethyl)-1,2-dihydro-3-quinolinecarboxylate; sodium glycinate; In ethanol; at 180 ℃; for 0.5h; Microwave;

With hydrogenchloride; In ethanol; water;