Benzenemethanol, alpha-(1-aminoethyl)-5-methoxy-2-methyl-, (R,S)- (9CI)

Base Information

Chemical Name:Benzenemethanol, alpha-(1-aminoethyl)-5-methoxy-2-methyl-, (R*,S*)- (9CI)
CAS No.:736868-96-5
Molecular Formula:C₁₁H₁₇NO₂
Molecular Weight:195.261
Hs Code.:
Mol file:736868-96-5.mol

Synonyms:Benzenemethanol,a-(1-aminoethyl)-5-methoxy-2-methyl-,(R*,S*)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, alpha-(1-aminoethyl)-5-methoxy-2-methyl-, (R*,S*)- (9CI)

Chemical Property:

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Technology Process of Benzenemethanol, alpha-(1-aminoethyl)-5-methoxy-2-methyl-, (R*,S*)- (9CI)

There total 3 articles about Benzenemethanol, alpha-(1-aminoethyl)-5-methoxy-2-methyl-, (R*,S*)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-24-3
Nitroethane

: 52289-54-0
4-methoxysalicylaldehyde

: 736868-96-5
C₈H₉OCHOHCHNH₂CH₃

: 736868-96-5
C₈H₉OCHOHCHNH₂CH₃

Guidance literature:: Nitroethane; 4-methoxysalicylaldehyde; With sodium hexamethyldisilazane; neodymium (III) isopropoxide; In tetrahydrofuran; water; at -40 ℃; for 48h;

With sodium tetrahydroborate; nickel dichloride; In methanol; at 0 ℃; Further stages. Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2007.11.055

Reference yield:

: 79-24-3
Nitroethane

: 52289-54-0
4-methoxysalicylaldehyde

: 736868-96-5
C₈H₉OCHOHCHNH₂CH₃

: 736868-96-5
C₈H₉OCHOHCHNH₂CH₃

Guidance literature:: Nitroethane; 4-methoxysalicylaldehyde; With sodium hexamethyldisilazane; neodymium (III) isopropoxide; In tetrahydrofuran; water; at -40 ℃; for 48h;

With sodium tetrahydroborate; nickel dichloride; In methanol; at 0 ℃; Further stages. Title compound not separated from byproducts.;
DOI:10.1016/j.tetlet.2007.11.055