(E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

Base Information

Chemical Name:(E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid
CAS No.:1021540-48-6
Molecular Formula:C₂₁H₁₉F₃O₆
Molecular Weight:424.373
Hs Code.:

Synonyms:(E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

Chemical Property:

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Technology Process of (E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

There total 3 articles about (E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116412-99-8
(3,4-dimethoxyphenyl)(4-(trifluoromethyl)phenyl)methanone

: 106-65-0
Dimethyl succinate

: 1021540-48-6
(E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; tert-butyl alcohol; for 3h; Reflux;
DOI:10.1080/07391102.2020.1764867

Reference yield:

: 455-24-3
4-trifluoromethylbenzoic acid

: 1021540-48-6
(E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: polyphosphoric acid / 5 h / 90 °C

2: 5,5-dimethyl-1,3-cyclohexadiene; tert-butyl alcohol / 3 h / Reflux

With polyphosphoric acid; In 5,5-dimethyl-1,3-cyclohexadiene; tert-butyl alcohol;
DOI:10.1080/07391102.2020.1764867

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 1021540-48-6
(E/Z)-3-methoxycarbonyl-4-(4-(trifluoromethyl)phenyl)-4-(3,4-dimethoxyphenyl)-3-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: polyphosphoric acid / 5 h / 90 °C

2: 5,5-dimethyl-1,3-cyclohexadiene; tert-butyl alcohol / 3 h / Reflux

With polyphosphoric acid; In 5,5-dimethyl-1,3-cyclohexadiene; tert-butyl alcohol;
DOI:10.1080/07391102.2020.1764867