C₂₇H₄₄O₂

Base Information

• Chemical Name: C₂₇H₄₄O₂
• CAS No.: 1383941-68-1
• Molecular Formula: C₂₇H₄₄O₂
• Molecular Weight: 400.645
• Mol file: 1383941-68-1.mol

Synonyms:C₂₇H₄₄O₂

Chemical Property of C₂₇H₄₄O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₄₄O₂

There total 3 articles about C₂₇H₄₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C29H46O3 (1383941-67-0) → C27H44O2 (1383941-68-1)

Guidance literature:

With sodium hydroxide; In isopropyl alcohol; at 80 ℃; for 5h; Inert atmosphere;

DOI:10.1007/s11164-012-0635-5

Reference yield:

(-)-8-[(p-methoxy)phenyl]menthol (80868-36-6) → C27H44O2 (1383941-68-1)

Guidance literature:

Multi-step reaction with 4 steps

1: dmap / pyridine / 20 °C / Inert atmosphere

2: boron tribromide / dichloromethane / -78 - -25 °C / Inert atmosphere

3: caesium carbonate / d₇-N,N-dimethylformamide / 3 h / 80 °C / Inert atmosphere

4: sodium hydroxide / isopropyl alcohol / 5 h / 80 °C / Inert atmosphere

With dmap; boron tribromide; caesium carbonate; sodium hydroxide; In pyridine; dichloromethane; d₇-N,N-dimethylformamide; isopropyl alcohol;

DOI:10.1007/s11164-012-0635-5

Reference yield:

Acetic acid (1R,2S,5R)-2-[1-(4-methoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexyl ester (680580-85-2) → C27H44O2 (1383941-68-1)

Guidance literature:

Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane / -78 - -25 °C / Inert atmosphere

2: caesium carbonate / d₇-N,N-dimethylformamide / 3 h / 80 °C / Inert atmosphere

3: sodium hydroxide / isopropyl alcohol / 5 h / 80 °C / Inert atmosphere

With boron tribromide; caesium carbonate; sodium hydroxide; In dichloromethane; d₇-N,N-dimethylformamide; isopropyl alcohol;

DOI:10.1007/s11164-012-0635-5

upstream raw materials:

(-)-8-[(p-methoxy)phenyl]menthol

C₂₉H₄₆O₃

Acetic acid (1R,2S,5R)-2-[1-(4-methoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexyl ester