3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Base Information

Chemical Name:3-azido-N-tert-butyl-N-hydroxylaminylbenzene
CAS No.:364038-68-6
Molecular Formula:C₁₀H₁₄N₄O
Molecular Weight:206.247
Hs Code.:

Synonyms:3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Suppliers and Price of 3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-azido-N-tert-butyl-N-hydroxylaminylbenzene

There total 3 articles about 3-azido-N-tert-butyl-N-hydroxylaminylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 749916-98-1
3-azido-N-tert-butyldimethylsiloxy-N-tert-butylaminobenzene

: 364038-68-6
3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 20 ℃;
DOI:10.1021/jo049500r

Reference yield:

: 108-36-1
1,3-dibromobenzene

: 364038-68-6
3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: BuLi

2.1: n-BuLi / diethyl ether; hexane / 1.25 h / -78 - 20 °C

2.2: 83 percent / tosyl azide / diethyl ether; hexane / 20 °C

3.1: 79 percent / tetrabutylammonium fluoride / tetrahydrofuran; CH₂Cl₂ / 20 °C

With n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo049500r

Reference yield:

: 233584-39-9
N-3-bromophenyl-N-tert-butyl-N-tert-butyldimethylsiloxyamine

: 364038-68-6
3-azido-N-tert-butyl-N-hydroxylaminylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / diethyl ether; hexane / 1.25 h / -78 - 20 °C

1.2: 83 percent / tosyl azide / diethyl ether; hexane / 20 °C

2.1: 79 percent / tetrabutylammonium fluoride / tetrahydrofuran; CH₂Cl₂ / 20 °C

With n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo049500r