1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine

Base Information

• Chemical Name: 1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine
• CAS No.: 1240659-45-3
• Molecular Formula: C₁₂H₁₇N₃O₂
• Molecular Weight: 235.286
• Mol file: 1240659-45-3.mol

Synonyms:1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine

Chemical Property of 1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine

There total 1 articles about 1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-(4'-nitrophenyl)butan-2-one (63099-53-6) + N,N-Dimethylhydrazine (57-14-7) → 1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine (1240659-45-3)

Guidance literature:

With sodium acetate; acetic acid; In ethanol; at 150 ℃; for 1h; Microwave irradiation;

DOI:10.1021/ol101130e

Reference yield:

1,1-dimethyl-2-(3-(4-nitrophenyl)butan-2-ylidene)hydrazine (1240659-45-3) + methyl iodide (74-88-4) → C13H20N3O2(1+)*I(1-)

Guidance literature:

In acetonitrile; at 20 ℃; for 20h;

DOI:10.1021/ol101130e

upstream raw materials:

3-(4'-nitrophenyl)butan-2-one

N,N-Dimethylhydrazine