2,6-di-tert-butylphenyl ethyl malonate

Base Information

Chemical Name:2,6-di-tert-butylphenyl ethyl malonate
CAS No.:1384252-77-0
Molecular Formula:C₁₉H₂₈O₄
Molecular Weight:320.429
Hs Code.:

Synonyms:2,6-di-tert-butylphenyl ethyl malonate

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Chemical Property of 2,6-di-tert-butylphenyl ethyl malonate

Chemical Property:

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Technology Process of 2,6-di-tert-butylphenyl ethyl malonate

There total 1 articles about 2,6-di-tert-butylphenyl ethyl malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1071-46-1
hydrogen ethyl malonate

: 128-39-2
2,6-di-tert-butylphenol

: 1384252-77-0
2,6-di-tert-butylphenyl ethyl malonate

Guidance literature:: With trichlorophosphate; In chloroform; at 20 ℃; for 8h; Reflux;
DOI:10.1039/c2cc32772d

Reference yield: 26.0%

: 1384252-77-0
2,6-di-tert-butylphenyl ethyl malonate

: 1384252-74-7
C₁₉H₂₈O₆

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; at 20 ℃; for 12h; Reflux;
DOI:10.1039/c2cc32772d

Reference yield:

: 1384252-77-0
2,6-di-tert-butylphenyl ethyl malonate

: 1384252-72-5
(3S,4R)-ethyl 4-benzyl-3-hydroxy-2-oxotetrahydrofuran-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: selenium(IV) oxide / 1,4-dioxane / 12 h / 20 °C / Reflux

2: 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole / toluene / 2 h / 20 °C

3: L-Selectride / tetrahydrofuran; dichloromethane / 1 h / -78 °C

4: hydrogenchloride / tetrahydrofuran; diethyl ether; dichloromethane / 1 h

With hydrogenchloride; selenium(IV) oxide; L-Selectride; 5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; toluene; 2: Aldol reaction;
DOI:10.1039/c2cc32772d