Technology Process of C40H68N2O9
There total 7 articles about C40H68N2O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 79 percent / NaH; tetramethylammonium iodide / tetrahydrofuran / 2 h / Heating
2: 88 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating
3: toluene; 2-methyl-propan-2-ol / 24 h / 130 - 150 °C
With
lithium aluminium tetrahydride; tertamethylammonium iodide; sodium hydride;
In
tetrahydrofuran; toluene; tert-butyl alcohol;
DOI:10.1021/ma049551q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 88 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating
2: toluene; 2-methyl-propan-2-ol / 24 h / 130 - 150 °C
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; toluene; tert-butyl alcohol;
DOI:10.1021/ma049551q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: oxalyl chloride; DMF / CH2Cl2 / 3 h / Heating
2: 81 percent / triethylamine / CH2Cl2 / 15 h / 20 °C
3: 79 percent / NaH; tetramethylammonium iodide / tetrahydrofuran / 2 h / Heating
4: 88 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating
5: toluene; 2-methyl-propan-2-ol / 24 h / 130 - 150 °C
With
lithium aluminium tetrahydride; oxalyl dichloride; tertamethylammonium iodide; sodium hydride; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1021/ma049551q