4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

Base Information

Chemical Name:4β-amino-4′-desmethylepipdophyllotoxin hydrochloride
CAS No.:1134455-96-1
Molecular Formula:C₂₁H₂₁NO₇*ClH
Molecular Weight:435.861
Hs Code.:

Synonyms:4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

Chemical Property:

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Technology Process of 4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

There total 1 articles about 4β-amino-4′-desmethylepipdophyllotoxin hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 150059-96-4
4β-chloroacetamido-4-deoxy-4′-desmethylepipdophyllotoxin

: 1134455-96-1
4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

Guidance literature:: With acetic acid; thiourea; at 80 ℃; Product distribution / selectivity;

Reference yield: 37.08%

: 1126-74-5
3-(pyridin-3-yl)acrylic acid

: 1134455-96-1
4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

: 4β-4-(3”-pyridineacrylamido)-4-deoxy-4′-desmethylepipdophyllotoxin

Guidance literature:: 3-(pyridin-3-yl)acrylic acid; With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;

4β-amino-4′-desmethylepipdophyllotoxin hydrochloride; In N,N-dimethyl-formamide;

Reference yield: 37.0%

: 6300-04-5
3-dimethylaminopropionic acid

: 1134455-96-1
4β-amino-4′-desmethylepipdophyllotoxin hydrochloride

: 3-dimethylamino-N-[9-(4-hydroxy-3,5-dimethoxyphenyl)-8-oxo-5,5a,6,8,8a,9-hexahydrofuro[3',4':6,7]naphtho[2,3-d][1,3]dioxol-5-yl]-propionamide hydrochloride

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In acetonitrile; at 20 ℃; for 6h;