1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

Base Information

Chemical Name:1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene
CAS No.:1160484-10-5
Molecular Formula:C₂₆H₂₄FeNO₃P
Molecular Weight:485.302
Hs Code.:

Synonyms:1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

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Chemical Property of 1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

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Technology Process of 1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

There total 1 articles about 1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 173346-69-5
1′-(diphenylphosphino)ferrocene-1-carboxylic acid

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 1160484-10-5
1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

Guidance literature:: With (CH₃)2NCH₂CH₂CH₂NCNCH₂CH₃; 1-hydroxybenzotriazole; N(CH₂CH₃)3; In dichloromethane; (Ar, dark); addn. of diimide deriv. to CH2Cl2 soln. of ferrocene deriv. and benzotriazole at 0°C, stirring at 0°C for 30 min, addn. of glycine deriv. and triethylamine in CH2Cl2, stirring overnight at room temp.; washing with aq. citric acid, satd. aq. NaHCO3 and brine, drying over MgSO4, evapn., chromy. (silica gel, CH2Cl2/methanol (10:1)), evapn., elem.anal.;
DOI:10.1021/om900209j

Reference yield: 98.0%

: 10544-50-0
sulfur

: 1160484-10-5
1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

: 1160484-17-2
1-diphenylthiophosphoryl-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

Guidance literature:: In ethyl acetate; (Ar, dark); refluxing soln. of ferrocene deriv. and sulphur in ethyl acetate for 90 min; cooling to room temp., evapn., chromy. (silica gel, CH2Cl2/methanol (20:1)), evapn., elem. anal.;
DOI:10.1021/om900209j

Reference yield: 97.0%

: (2-methylallyl)palladium-chloride dimer

: 1160484-10-5
1-diphenylphosphino-1'-(N-[(methoxycarbonyl)methyl]carbamoyl)ferrocene

: 109-66-0,8031-35-4,9078-70-0
pentane

: [(η3-C3H4Me)PdCl((Ph2PC5H4)Fe(C5H4C(O)NHCH2CO2Me)-κP)2]ClO4*0.5C5H12

Guidance literature:: In chloroform; byproducts: CH3CN; (Ar); exclusion of direct daylight; soln. of Fe complex (2 equiv.) in CHCl3 was added to Pd complex (1 equiv.); stirred at room temp. for 1 h; poured into pentane; kept at -18°C overnight; filtered; washed (pentane); dried (vac.); elem. anal.;
DOI:10.1039/c1dt11230a