C₁₅H₁₅ClN₂O₂S

Base Information

Chemical Name:C₁₅H₁₅ClN₂O₂S
CAS No.:1232770-29-4
Molecular Formula:C₁₅H₁₅ClN₂O₂S
Molecular Weight:322.815
Hs Code.:

C<sub>15</sub>H<sub>15</sub>ClN<sub>2</sub>O<sub>2</sub>S

Synonyms:C₁₅H₁₅ClN₂O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₅ClN₂O₂S

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Technology Process of C₁₅H₁₅ClN₂O₂S

There total 5 articles about C₁₅H₁₅ClN₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-18-6
formic acid

: 1228150-27-3
C₁₄H₁₅ClN₂OS

: 1232770-29-4
C₁₅H₁₅ClN₂O₂S

Guidance literature:: formic acid; With acetic anhydride; at 60 ℃; for 1h; Inert atmosphere;

C₁₄H₁₅ClN₂OS; for 2h; Cooling with ice;

Reference yield:

: 6258-60-2
p-methoxybenzylmercaptan

: 1232770-29-4
C₁₅H₁₅ClN₂O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 3 h / 25 °C / Inert atmosphere

2.1: trichlorophosphate; N,N-diethylaniline / 3 h / Reflux

3.1: tin(II) chloride dihdyrate; hydrogenchloride / water; diethyl ether / 2 h / 25 °C

4.1: acetic anhydride / 1 h / 60 °C / Inert atmosphere

4.2: 2 h / Cooling with ice

With hydrogenchloride; tin(II) chloride dihdyrate; acetic anhydride; sodium hydride; N,N-diethylaniline; trichlorophosphate; In tetrahydrofuran; diethyl ether; water; mineral oil;

Reference yield:

: C₁₄H₁₄N₂O₄S

: 1232770-29-4
C₁₅H₁₅ClN₂O₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate; N,N-diethylaniline / 3 h / Reflux

2.1: tin(II) chloride dihdyrate; hydrogenchloride / water; diethyl ether / 2 h / 25 °C

3.1: acetic anhydride / 1 h / 60 °C / Inert atmosphere

3.2: 2 h / Cooling with ice

With hydrogenchloride; tin(II) chloride dihdyrate; acetic anhydride; N,N-diethylaniline; trichlorophosphate; In diethyl ether; water;