Technology Process of 4-benzyl-10,16-diethyl-4,10,16-triaza-1,7,13-trioxacyclooctadecane
There total 5 articles about 4-benzyl-10,16-diethyl-4,10,16-triaza-1,7,13-trioxacyclooctadecane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 24h;
Heating;
DOI:10.1021/jo00278a016
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride
2: 71 percent / anhydrous Na2CO3 / toluene / 48 h / Heating
3: 73 percent / LiAlH4 / tetrahydrofuran
4: 62 percent / triethylamine / toluene / 24 h / Ambient temperature
5: 74 percent / LiAlH4
With
lithium aluminium tetrahydride; thionyl chloride; sodium carbonate; triethylamine;
In
tetrahydrofuran; toluene;
DOI:10.1016/0040-4039(88)85282-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 71 percent / anhydrous Na2CO3 / toluene / 48 h / Heating
2: 73 percent / LiAlH4 / tetrahydrofuran
3: 62 percent / triethylamine / toluene / 24 h / Ambient temperature
4: 74 percent / LiAlH4
With
lithium aluminium tetrahydride; sodium carbonate; triethylamine;
In
tetrahydrofuran; toluene;
DOI:10.1016/0040-4039(88)85282-1
