10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

Base Information

Chemical Name:10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione
CAS No.:118974-49-5
Molecular Formula:C₂₃H₃₇N₃O₅
Molecular Weight:435.564
Hs Code.:

Synonyms:10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

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Chemical Property of 10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

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Technology Process of 10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

There total 4 articles about 10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 21062-20-4
diglycolyl chloride

: 118974-42-8
9-benzyl-3,9,15-triaza-6,12-dioxaheptadecane

: 118974-49-5
10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

Guidance literature:: With triethylamine; In toluene; for 24h; Ambient temperature;
DOI:10.1016/0040-4039(88)85282-1

Reference yield:

: 118974-46-2
N-[2-(2-hydroxyethoxy)ethyl]acetamide

: 118974-49-5
10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: 71 percent / anhydrous Na₂CO₃ / toluene / 48 h / Heating

3: 73 percent / LiAlH₄ / tetrahydrofuran

4: 62 percent / triethylamine / toluene / 24 h / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; sodium carbonate; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/0040-4039(88)85282-1

Reference yield:

: 118974-47-3
N-[2-(2-chloroethoxy)ethyl]acetamide. N-[2-(2-hydroxyethoxy)ethyl]acetamide

: 118974-49-5
10-Benzyl-4,16-diethyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadecane-3,17-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / anhydrous Na₂CO₃ / toluene / 48 h / Heating

2: 73 percent / LiAlH₄ / tetrahydrofuran

3: 62 percent / triethylamine / toluene / 24 h / Ambient temperature

With lithium aluminium tetrahydride; sodium carbonate; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/0040-4039(88)85282-1