3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

Base Information

Chemical Name:3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl
CAS No.:76893-42-0
Molecular Formula:C₁₅H₁₈N₃O₅S
Molecular Weight:352.391
Hs Code.:

Synonyms:3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

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Chemical Property of 3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

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Technology Process of 3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

There total 3 articles about 3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 76893-40-8
S-(1-Oxyl-2,2,5,5-tetramethyl-2,5-dihydropyrrol-3-ylmethyl)-thiuronium methanesulfonate

: 76893-42-0
3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

Guidance literature:: With sodium hydroxide; In ethanol; Ambient temperature;
DOI:10.1055/s-1980-29269

Reference yield:

: 55738-75-5
(2,5-dihydro-2,2,5,5-tetramethyl-1-oxyl-1H-pyrrol-3-yl)methanol

: 76893-42-0
3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

2: 75 percent / acetone / 0.25 h / Heating

3: 90 percent / NaOH / aq. ethanol / Ambient temperature

With sodium hydroxide; triethylamine; In ethanol; dichloromethane; acetone;
DOI:10.1055/s-1980-29269

Reference yield:

: 76893-27-1
(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-yl)methyl methanesulfonate

: 76893-42-0
3-(2,4-Dinitrophenylthiomethyl)-2,2,5,5-tetramethyl-2,5-dihydropyrrole-1-oxyl

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetone / 0.25 h / Heating

2: 90 percent / NaOH / aq. ethanol / Ambient temperature

With sodium hydroxide; In ethanol; acetone;
DOI:10.1055/s-1980-29269