Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2

Base Information

Chemical Name:Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2
CAS No.:89530-56-3
Molecular Formula:C₅₁H₄₇Cl₅OP₄Re₂
Molecular Weight:1349.51
Hs Code.:

Synonyms:Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2

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Chemical Property of Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2

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Technology Process of Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2

There total 1 articles about Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 14023-10-0
tetra-n-butylammonium octachlorodirhenate(III)

: 2071-20-7
bis-diphenylphosphinomethane

: 58312-74-6
Re₂(μ-dppm)₂(μ-Cl)₂Cl₄

: 89530-56-3
Re2(μ-Cl)2Cl3(OMe)(bis(diphenylphosphino)methane)2

Guidance literature:: With methanol; In methanol; diethyl ether; under N2, mixt. of reagents refluxed in mixt. of reagent grade MeOH anddry Et2O for 30 min with rapid stirring; solid filtered off, dissolved in toluene-CH2Cl2, allowed to stand for 2h, filtered, evapd., recrystd. from CH2Cl2 by slow addn. of Et2O; elem.anal.;
DOI:10.1021/ja00322a024