Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI)

Base Information

• Chemical Name: Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI)
• CAS No.: 731772-97-7
• Molecular Formula: C₁₀H₁₁F
• Molecular Weight: 150.196
• Hs Code.: 2903999090
• Mol file: 731772-97-7.mol

Synonyms:Benzene,1-fluoro-2-(2-methyl-2-propenyl)- (9CI)

Chemical Property of Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI)

Chemical Property:

• Vapor Pressure: 1.15mmHg at 25°C
• Refractive Index: 1.489
• Boiling Point: 181.6°C at 760 mmHg
• Flash Point: 55.4°C
• PSA: 0.00000
• Density: 0.972g/cm³
• LogP: 2.94430

Purity/Quality:

97% ^*data from raw suppliers

3-(2-fluorophenyl)-2-methyl-1-propene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI)

There total 1 articles about Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

fluorobenzene (462-06-6) + 3-Chloro-2-methylpropene (563-47-3) → 1-fluoro-2-(2-methylallyl)benzene (731772-97-7)

Guidance literature:

With di-tert-butyl(2-methoxyphenyl)phosphine; palladium diacetate; silver pivalate; caesium carbonate; In neat (no solvent); at 120 ℃; for 17h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/jacs.6b10220

upstream raw materials:

fluorobenzene

3-Chloro-2-methylpropene

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