bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate

Base Information

• Chemical Name: bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate
• CAS No.: 100225-45-4
• Molecular Formula: C₃₃H₃₁IMoP₂*F₆P
• Molecular Weight: 857.365

Synonyms:bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate

Chemical Property of bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate

Chemical Property:

Purity/Quality:

99% ，98% ^*data from raw suppliers

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Technology Process of bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate

There total 2 articles about bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ammonium hexafluorophosphate + MoI(Ph2PCH2CH2PPh2)(η-cycloheptatrienyl) → bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate (100225-45-4)

Guidance literature:

With I₂; In water; acetone; toluene; treating with 1 equiv of I2 in toluene under N2 to give a black ppt., sepg., extg. with aq. acetone, filtering, addn. of aq. NH4PF6 to the filtrate; concn., recrystallization from CH2Cl2-petroleum ether, elem. anal.;

DOI:10.1016/S0277-5387(00)84077-2

Reference yield: 35.0%

(acetone){1,2-bis(diphenylphosphino)ethane}(η-cycloheptatrienyl)molybdenum(1+) hexafluorophosphate + lithium iodide (10377-51-2) → bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)iodomolybdenum hexafluorophosphate (100225-45-4)

Guidance literature:

In acetone; (N2); reflux (4 h); filtration, evapn. to dryness (vac.), recrystn. (CH2Cl2/Et2O); elem. anal.;

DOI:10.1039/a907205e

upstream raw materials:

lithium iodide

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