6-Bromo-2-methylimidazo[1,2-a]pyridine-3-carbaldehyde

Base Information

• Chemical Name: 6-Bromo-2-methylimidazo[1,2-a]pyridine-3-carbaldehyde
• CAS No.: 728864-58-2
• Molecular Formula: C9H7 Br N2 O
• Molecular Weight: 239.071
• Hs Code.: 2933990090
• DSSTox Substance ID: DTXSID40373720
• Wikidata: Q82162029
• Mol file: 728864-58-2.mol

Synonyms:728864-58-2;6-bromo-2-methylimidazo[1,2-a]pyridine-3-carbaldehyde;6-Bromo-2-methyl-imidazo[1,2-a]pyridine-3-carbaldehyde;6-Bromo-2-methylimidazo-[1,2-a]pyridine-3-carbaldehyde;SCHEMBL2457745;DTXSID40373720;UVICLOBRWKMASM-UHFFFAOYSA-N;AKOS017553010;AB20703;FS-6172;CS-0099581;FT-0731401;EN300-6498899;A866185;A1-08783;6-Bromo-2-methylimidazo[1,2-a]pyridine-3-carboxaldehyde

Chemical Property of 6-Bromo-2-methylimidazo[1,2-a]pyridine-3-carbaldehyde

Chemical Property:

• PSA: 34.37000
• LogP: 2.21770
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 237.97418
• Heavy Atom Count: 13
• Complexity: 212

Purity/Quality:

97% ^*data from raw suppliers

6-Bromo-2-methylimidazo-[1,2-a]pyridine-3-carbaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(N2C=C(C=CC2=N1)Br)C=O

Technology Process of 6-Bromo-2-methylimidazo[1,2-a]pyridine-3-carbaldehyde

There total 3 articles about 6-Bromo-2-methylimidazo[1,2-a]pyridine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromo-2-methylimidazo[1,2-a]pyridine (4044-99-9) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 6-bromo-2-methylimidazo [1,2-a]pyridine-3-carbaldehyde (728864-58-2)

Guidance literature:

N,N-dimethyl-formamide; With trichlorophosphate; at 0 ℃; for 0.0833333h;

6-bromo-2-methylimidazo[1,2-a]pyridine; at 50 ℃; for 6h;

Reference yield:

6-bromo-2-methylimidazo[1,2-a]pyridine (4044-99-9) + Vilsmeier reagent (3724-43-4,149409-22-3) → 6-bromo-2-methylimidazo [1,2-a]pyridine-3-carbaldehyde (728864-58-2)

Guidance literature:

Vilsmeier reagent; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

6-bromo-2-methylimidazo[1,2-a]pyridine; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 1h;

Reference yield:

5-bromo-2-pyridylamine (1072-97-5) → 6-bromo-2-methylimidazo [1,2-a]pyridine-3-carbaldehyde (728864-58-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 20 h / 90 °C

2.1: N,N-dimethyl-formamide / 0.08 h / 0 °C

2.2: 1 h / 20 - 80 °C

In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

6-bromo-2-methylimidazo[1,2-a]pyridine

Vilsmeier reagent

5-bromo-2-pyridylamine

N,N-dimethyl-formamide

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