tetrahydridododecacarbonyltetraruthenium

Base Information

Chemical Name:tetrahydridododecacarbonyltetraruthenium
CAS No.:34438-91-0
Molecular Formula:12CO*H₄Ru₄
Molecular Weight:744.437
Hs Code.:

Synonyms:tetrahydridododecacarbonyltetraruthenium

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Chemical Property of tetrahydridododecacarbonyltetraruthenium

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Technology Process of tetrahydridododecacarbonyltetraruthenium

There total 29 articles about tetrahydridododecacarbonyltetraruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.9%

: 86276-91-7,117307-98-9
Ru₃(CO)11(P(C₆H₅)(OCH₃)2)

: 34438-91-0,1149341-24-1,1149341-22-9,1149341-27-4,1149341-23-0
[Ru4(μ-H)4(CO)12]

: Ru₄H₄(CO)10(P(C₆H₅)(OCH₃)2)2

: Ru₄H₄(CO)11(P(C₆H₅)(OCH₃)2)

: Ru₄H₄(CO)9(P(C₆H₅)(OCH₃)2)3

Guidance literature:: With H₂; In cyclohexane; High Pressure; hydrogenated in an autoclave for 2 h at 80°C, at p(H2) 20 atm; cooled, evapd., dissolved in CH2Cl2, preparative TLC, identified from IR and TLC, elem. anal.;
DOI:10.1016/0022-328X(86)82088-5

Reference yield: 35.0%

: 39774-25-9
6-phenylpyridin-2-amine

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 34438-91-0
tetrahydridododecacarbonyltetraruthenium

: [Ru6(μ3-H)(μ5-η3-apyC6H4-N,N,C)(μ-CO)3(CO)13]

: [Ru6(μ3-H)2(μ5-η2-apyPh-N,N)(μ-CO)2(CO)14]

: [Ru3(μ-H)2(μ3-η3-HapyC6H4-N,N,C)2(CO)6]

Guidance literature:: In xylene; under N2 atm. soln. (Ru3(CO)12) and H2apyPh in xylene was heated at reflux temp. for 30 min; solvent was removed in vacuo, residue was dissolved in CH2Cl2 and chromed. on silica (hexane-Et2O); elem. anal.;
DOI:10.1021/om034040y