6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

Base Information

Chemical Name:6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline
CAS No.:1310575-31-5
Molecular Formula:C₂₃H₂₆N₂O₂
Molecular Weight:362.472
Hs Code.:

Synonyms:6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

Suppliers and Price of 6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

Chemical Property:

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Technology Process of 6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

There total 5 articles about 6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6-ethyl-1-(3-methoxyphenyl)-2,3,4,9-tetrahydro-1H-β-carboline

: 79-03-8
propionyl chloride

: 1310575-31-5
6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: With potassium carbonate; In water; ethyl acetate; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2011.03.048

Reference yield:

: 136281-75-9
(5-ethyl-1H-indol-3-yl)acetonitrile

: 1310575-31-5
6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether

2: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

3: potassium carbonate / water; ethyl acetate / 3 h / 0 - 20 °C

With lithium aluminium tetrahydride; potassium carbonate; trifluoroacetic acid; In diethyl ether; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.03.048

Reference yield:

: 62500-88-3
2-(5-ethyl-1H-indol-3-yl)ethylamine

: 1310575-31-5
6-ethyl-1-(3-methoxyphenyl)-2-propionyl-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

2: potassium carbonate / water; ethyl acetate / 3 h / 0 - 20 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.03.048