3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

Base Information

Chemical Name:3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid
CAS No.:632624-95-4
Molecular Formula:C₂₇H₂₃ClN₂O₄
Molecular Weight:474.944
Hs Code.:

Synonyms:3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

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Chemical Property of 3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

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Technology Process of 3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

There total 6 articles about 3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid methyl ester

: 632624-95-4
3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

Guidance literature:: With sodium hydroxide; water; In ethanol; at 120 ℃; for 0.05h; Microwave;

Reference yield:

: 5409-45-0
2-acetylamino-5-nitrobenzoic acid methyl ester

: 632624-95-4
3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 5%-palladium/activated carbon / methanol / 3 h / 20 °C / 760.05 Torr

2: toluene-4-sulfonic acid / 1-methyl-pyrrolidin-2-one / 0.17 h / 150 °C / Microwave

3: sodium hydroxide; water / ethanol / 0.05 h / 120 °C / Microwave

With sodium hydroxide; water; hydrogen; 5%-palladium/activated carbon; toluene-4-sulfonic acid; In 1-methyl-pyrrolidin-2-one; methanol; ethanol;

Reference yield:

: 38544-16-0
2-(benzyloxy)-5-chlorobenzaldehyde

: 632624-95-4
3-{2-[5-chloro-2-(benzyloxy)phenyl]-5-methyl-pyrrol-1-yl}-6-acetylaminobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine / ethanol / 5 h / Heating / reflux

2: toluene-4-sulfonic acid / 1-methyl-pyrrolidin-2-one / 0.17 h / 150 °C / Microwave

3: sodium hydroxide; water / ethanol / 0.05 h / 120 °C / Microwave

With sodium hydroxide; water; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine; toluene-4-sulfonic acid; In 1-methyl-pyrrolidin-2-one; ethanol;