(4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

Base Information

Chemical Name:(4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine
CAS No.:1398227-60-5
Molecular Formula:C₂₃H₂₉N₃O₂
Molecular Weight:379.502
Hs Code.:

Synonyms:(4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

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Chemical Property of (4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

Chemical Property:

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Technology Process of (4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

There total 1 articles about (4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 360054-69-9
(4R,5R)-1,3-dimethyl-4,5-(diphenyl)-imidazolidin-2-one

: 1398227-60-5
(4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / benzene / 9 h / 80 °C / Inert atmosphere

2: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; In dichloromethane; benzene;
DOI:10.1021/jo301178b

Reference yield: 95.0%

: 1398227-60-5
(4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

: 100-39-0
benzyl bromide

: (4R,5R)-2-{N-benzyl-[(tert-butoxycarbonyl)methyl]iminio}-1,3-dimethyl-4,5-diphenylimidazolidin Bromide

Guidance literature:: In acetonitrile; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo301178b

Reference yield:

: 1398227-60-5
(4R,5R)-2-[(tert-butoxycarbonyl)methyl]imino-1,3-dimethyl-4,5-diphenylimidazolidine

: 1398228-30-2
tert-butyl (2S,3R,4R,5R)-1-benzyl-3-hydroxy-5-hydroxymethyl-4-iodopyrrolidine-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 12 h / 20 °C / Inert atmosphere

2: N,N,N',N'-tetramethylguanidine / tetrahydrofuran / 16.5 h / 20 °C

3: toluene-4-sulfonic acid / tetrahydrofuran; water / 15 h / 20 °C

4: iodine; potassium carbonate / tetrahydrofuran / 2 h / -35 °C

With iodine; potassium carbonate; toluene-4-sulfonic acid; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jo301178b