3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

Base Information

Chemical Name:3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one
CAS No.:79878-77-6
Molecular Formula:C₁₉H₁₇N₃O₂S
Molecular Weight:351.429
Hs Code.:

Synonyms:3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

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Chemical Property of 3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

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Technology Process of 3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

There total 1 articles about 3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 17451-21-7
4-(4-methoxyphenyl)-2-oxo-3-butenoic acid

: 13278-67-6
4-(4-methylphenyl)-3-thiosemicarbazide

: 79878-77-6
3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

Guidance literature:: In ethanol; for 8h; Heating;

Reference yield: 65.0%

: 79878-77-6
3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

: 74-88-4
methyl iodide

: 79878-80-1
6-[(E)-2-(4-Methoxy-phenyl)-vinyl]-3-methylsulfanyl-4-p-tolyl-4H-[1,2,4]triazin-5-one

Guidance literature:: With sodium methylate; In methanol; overnight;

Reference yield:

: 79878-77-6
3-Mercapto-6-[(E)-2-(4-methoxy-phenyl)-vinyl]-4-p-tolyl-4H-[1,2,4]triazin-5-one

: 106-49-0,12221-03-3
p-toluidine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / sodium methoxide / methanol / overnight

2: 89 percent / 10N HCl / ethanol / 1 h / Heating

3: 80percent hydrazine hydrate / ethanol / 3.5 h / Heating

With hydrogenchloride; sodium methylate; hydrazine hydrate; In methanol; ethanol;