1-CYANO-3-(4-METHOXYPHENYL)-2-METHYLISOTHIOUREA

Base Information

• Chemical Name: 1-CYANO-3-(4-METHOXYPHENYL)-2-METHYLISOTHIOUREA
• CAS No.: 75565-12-7
• Molecular Formula: C₁₀H₁₁N₃OS
• Molecular Weight: 221.283
• Mol file: 75565-12-7.mol

Synonyms:Pseudourea,1-cyano-3-(p-methoxyphenyl)-2-methyl-2-thio- (7CI);Pseudourea, 3-cyano-1-(p-methoxyphenyl)-2-methyl-2-thio-(6CI);

Chemical Property of 1-CYANO-3-(4-METHOXYPHENYL)-2-METHYLISOTHIOUREA

Chemical Property:

• Boiling Point: 357.3oC at 760 mmHg
• Flash Point: 169.9oC
• PSA: 82.71000
• Density: 1.16g/cm3
• LogP: 2.38018

Purity/Quality:

97% ^*data from raw suppliers

1-CYANO-3-(4-METHOXYPHENYL)-2-METHYLISOTHIOUREA 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-CYANO-3-(4-METHOXYPHENYL)-2-METHYLISOTHIOUREA

There total 4 articles about 1-CYANO-3-(4-METHOXYPHENYL)-2-METHYLISOTHIOUREA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-aniline (104-94-9) + dimethyl N-cyanodithioiminocarbonate (10191-60-3) → N'-Cyan-N-(4-methoxy-phenyl)-S-methyl-isothioharnstoff (75565-12-7)

Guidance literature:

In methanol; for 3h; Reflux;

DOI:10.1016/j.tetlet.2013.07.158

Reference yield:

methyl iodide (74-88-4) → N-cyano-N'-(4-methoxy-phenyl)-S-methyl-isothiourea (75565-12-7)

Guidance literature:

Reference yield:

→ N'-Cyan-N-(4-methoxy-phenyl)-S-methyl-isothioharnstoff (75565-12-7)

Guidance literature:

(CH3-S)2C=N-CN, p-Anisidin, A., sd.;

DOI:10.1039/jr9630003327

upstream raw materials:

4-methoxy-aniline

dimethyl N-cyanodithioiminocarbonate

methyl iodide

Downstream raw materials:

7-amino-2-(4-methoxyphenylamino)-1,2,4-triazolo[1,5-a][1,3,5]triazine

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