potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate

Base Information

• Chemical Name: potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate
• CAS No.: 132573-84-3
• Molecular Formula: C₁₀H₁₁N₂O₂S₂*K
• Molecular Weight: 294.44
• Mol file: 132573-84-3.mol

Synonyms:potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate

Chemical Property of potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate

There total 4 articles about potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

carbon disulfide (75-15-0,12122-00-8) + 2-(4-methoxyphenyl)acetic acid hydrazide (57676-49-0) → potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate (132573-84-3)

Guidance literature:

With potassium hydroxide; In ethanol; for 16h;

DOI:10.1002/jhet.3513

Reference yield:

4-Methoxyphenylacetic acid (104-01-8) → potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate (132573-84-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid / Reflux

2: hydrazine hydrate / methanol / Reflux

3: potassium hydroxide / methanol / 0 - 5 °C

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In methanol;

DOI:10.1590/S0103-50532012000500010

Reference yield:

4-methoxy-phenyl acetic acid methyl ester (23786-14-3) → potassium 2-[2-(4-methoxyphenyl)acetyl]hydrazinecarbodithioate (132573-84-3)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / Reflux

2: potassium hydroxide / methanol / 0 - 5 °C

With hydrazine hydrate; potassium hydroxide; In methanol;

DOI:10.1590/S0103-50532012000500010

upstream raw materials:

carbon disulfide

2-(4-methoxyphenyl)acetic acid hydrazide

4-Methoxyphenylacetic acid

4-methoxy-phenyl acetic acid methyl ester

Downstream raw materials:

4-amino-3-(4-methoxybenzyl)-1H-1,2,4-triazole-5(4H)-thione

C₁₇H₁₂F₂N₄OS

6-(4-Chloro-phenyl)-3-(4-methoxy-benzyl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

3-(4-methoxybenzyl)-6-(4-fluorophenyl)-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole