bis(3,5-dimethylphenyl)phosphinic amide

Base Information

Chemical Name:bis(3,5-dimethylphenyl)phosphinic amide
CAS No.:1201903-43-6
Molecular Formula:C₁₆H₂₀NOP
Molecular Weight:273.315
Hs Code.:

Synonyms:bis(3,5-dimethylphenyl)phosphinic amide

Suppliers and Price of bis(3,5-dimethylphenyl)phosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(3,5-dimethylphenyl)phosphinic amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(3,5-dimethylphenyl)phosphinic amide

There total 3 articles about bis(3,5-dimethylphenyl)phosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 137219-82-0
Bis(3,5-dimethylphenyl)phosphinic acid

: 1201903-43-6
bis(3,5-dimethylphenyl)phosphinic amide

Guidance literature:: Bis(3,5-dimethylphenyl)phosphinic acid; With thionyl chloride; In toluene; at 55 - 60 ℃; for 0.333333h;

With ammonia; In toluene; at -20 ℃;

Reference yield:

: 137219-83-1
(3-(chloro(3,5-dimethylphenyl)phosphoryl)-5-methylphenyl)methylium

: 1201903-43-6
bis(3,5-dimethylphenyl)phosphinic amide

Guidance literature:: With ammonia; In toluene; at 0 ℃; for 0.166667h;
DOI:10.1021/cm201940f

Reference yield:

: 556-96-7
5-bromo-1,3-xylene

: 1201903-43-6
bis(3,5-dimethylphenyl)phosphinic amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / 20 °C

1.2: 20 °C

1.3: 1 h / 80 °C

2.1: thionyl chloride / toluene / 55 - 60 °C

3.1: ammonia / toluene / 0.17 h / 0 °C

With thionyl chloride; ammonia; magnesium; In tetrahydrofuran; toluene;
DOI:10.1021/cm201940f