2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone

Base Information Edit

Chemical Name:2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone
CAS No.:951386-29-1
Molecular Formula:C₂₅H₃₂O₂Si
Molecular Weight:392.613
Hs Code.:
Mol file:951386-29-1.mol

Synonyms:2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone

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Chemical Property of 2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone Edit

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Technology Process of 2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone

There total 1 articles about 2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 130745-59-4
4-<(tert-Butyldiphenylsilyl)oxy>cyclohexanone

: 67-64-1
acetone

: 951386-29-1
2-isopropylidene-4-(tert-butyldiphenylsilyloxy)cyclohexanone

Guidance literature:: 4-<(tert-Butyldiphenylsilyl)oxy>cyclohexanone; acetone; With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In tetrahydrofuran; at -78 ℃; for 0.5h;

With toluene-4-sulfonic acid; In benzene; for 2h; Further stages.; Heating;
DOI:10.1021/jo071156l