Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

Base Information

Chemical Name:Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester
CAS No.:148680-21-1
Molecular Formula:C₁₅H₁₆N₂O₆
Molecular Weight:320.302
Hs Code.:

Synonyms:Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

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Chemical Property of Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

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Technology Process of Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

There total 12 articles about Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: Acetic acid (S)-5-methoxy-1-(3-methoxy-2-nitro-benzoyl)-pyrrolidin-2-ylmethyl ester

: 148680-21-1
Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

Guidance literature:: With quinolinium camphor-10-sulfonate; In toluene; Heating;
DOI:10.1016/S0040-4039(00)60643-3

Reference yield:

: 148680-18-6
L-2-(benzyloxycarbonylamino)-5,5-dimethoxypentanoic acid methyl ester

: 148680-21-1
Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / 10 percent Pd/C / ethanol / 3 h / 23 °C / 760 Torr

2: 95 percent / satd. aq. NaHCO₃ / CH₂Cl₂ / 23 °C

3: LiBH₄, LiBEt₃H / tetrahydrofuran / 1.33 h / 23 °C

4: pyridine / 0.25 h / 23 °C

5: camphorsulfonic acid, quinoline / benzene / 1.5 h / Heating

With pyridine; quinoline; lithium borohydride; camphor-10-sulfonic acid; hydrogen; lithium triethylborohydride; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1016/S0040-4039(00)77629-5

Reference yield:

: 148680-17-5
L-3-(benzyloxycarbonyl)-4-(3,3-dimethoxypropyl)-1,3-oxazolidin-5-one

: 148680-21-1
Acetic acid (S)-1-(3-methoxy-2-nitro-benzoyl)-2,3-dihydro-1H-pyrrol-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: sodium methoxide / 1.17 h / 23 °C

2: hydrogen / 10 percent Pd/C / ethanol / 3 h / 23 °C / 760 Torr

3: 95 percent / satd. aq. NaHCO₃ / CH₂Cl₂ / 23 °C

4: LiBH₄, LiBEt₃H / tetrahydrofuran / 1.33 h / 23 °C

5: pyridine / 0.25 h / 23 °C

6: camphorsulfonic acid, quinoline / benzene / 1.5 h / Heating

With pyridine; quinoline; lithium borohydride; camphor-10-sulfonic acid; hydrogen; sodium methylate; lithium triethylborohydride; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1016/S0040-4039(00)77629-5