Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside

Base Information

Chemical Name:Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside
CAS No.:220587-68-8
Molecular Formula:C₁₄H₁₈O₄Se
Molecular Weight:329.255
Hs Code.:
DSSTox Substance ID:DTXSID301182597
Nikkaji Number:J1.099.010F

Synonyms:DTXSID301182597;Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside;1-(Phenylseleno)-2-O,3-O-isopropylidene-1-deoxy-beta-D-ribofuranose;220587-68-8

Suppliers and Price of Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:330.03703
Heavy Atom Count:19
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(OC2C(OC(C2O1)[Se]C3=CC=CC=C3)CO)C
Isomeric SMILES:CC1(O[C@@H]2[C@H](O[C@H]([C@@H]2O1)[Se]C3=CC=CC=C3)CO)C

Technology Process of Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside

There total 4 articles about Phenyl 2,3-O-(1-methylethylidene)-1-seleno-beta-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 67-64-1
acetone

: 220588-06-7
phenyl 1-seleno-β-D-ribofuranoside

: 220587-68-8
phenyl 2,3-O-isopropylidene-1-seleno-β-D-ribofuranoside

Guidance literature:: With toluene-4-sulfonic acid; for 5h;
DOI:10.1021/jo981435w

Reference yield:

: 645-96-5
Benzeneselenol

: 220587-68-8
phenyl 2,3-O-isopropylidene-1-seleno-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / BF₃*Et₂O

2: 91 percent / K₂CO₃ / tetrahydrofuran; methanol / 6 h

3: 92 percent / p-MeC₆H₄SO₃H*H₂O / 5 h

With boron trifluoride diethyl etherate; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jo981435w

Reference yield:

: 74458-63-2
phenyl 2,3,5-tri-O-acetyl-1-seleno-β-D-ribofuranoside

: 220587-68-8
phenyl 2,3-O-isopropylidene-1-seleno-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / K₂CO₃ / tetrahydrofuran; methanol / 6 h

2: 92 percent / p-MeC₆H₄SO₃H*H₂O / 5 h

With potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jo981435w