C₃₅H₃₁F₂N₅O₆

Base Information

Chemical Name:C₃₅H₃₁F₂N₅O₆
CAS No.:1346567-70-1
Molecular Formula:C₃₅H₃₁F₂N₅O₆
Molecular Weight:655.658
Hs Code.:

C<sub>35</sub>H<sub>31</sub>F<sub>2</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₃₅H₃₁F₂N₅O₆

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Chemical Property of C₃₅H₃₁F₂N₅O₆

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Technology Process of C₃₅H₃₁F₂N₅O₆

There total 7 articles about C₃₅H₃₁F₂N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 1309832-72-1
1-(2,6-difluoro-phenyl)-1,4-dihydro-tetrazol-5-one

: 1346567-69-8
C₂₇H₂₉NO₄

: 1346567-70-1
C₃₅H₃₁F₂N₅O₆

Guidance literature:: bis(trichloromethyl) carbonate; C₂₇H₂₉NO₄; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.25h;

1-(2,6-difluoro-phenyl)-1,4-dihydro-tetrazol-5-one; With dmap; In toluene; for 2h; Reflux;

Reference yield:

: 65295-69-4
2,6-difluorophenyl isocyanate

: 1346567-70-1
C₃₅H₃₁F₂N₅O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylsilylazide / 12 h / Reflux

2.1: triethylamine / dichloromethane / 0.25 h / 0 - 20 °C

2.2: 2 h / Reflux

With trimethylsilylazide; triethylamine; In dichloromethane;

Reference yield:

: 151793-17-8
methyl 4-fluoro-2-methoxy-5-nitrobenzoate

: 1346567-70-1
C₃₅H₃₁F₂N₅O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1.5 h / 60 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere

4.1: zinc; acetic acid / tetrahydrofuran / 1 h / 0 °C

5.1: sodium tetrahydroborate; acetic acid / 1 h / 20 °C

6.1: triethylamine / dichloromethane / 0.25 h / 0 - 20 °C

6.2: 2 h / Reflux

With sodium tetrahydroborate; water; potassium carbonate; acetic acid; triethylamine; lithium hydroxide; zinc; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;