3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

Base Information

Chemical Name:3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester
CAS No.:152608-82-7
Molecular Formula:C₁₈H₂₇NO₅
Molecular Weight:337.416
Hs Code.:

Synonyms:3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

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Chemical Property of 3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

Chemical Property:

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Technology Process of 3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

There total 6 articles about 3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-(2,2-Diethoxy-chroman-5-yloxy)-pentanoic acid dimethylamide

: 152608-82-7
3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 1h; Yield given; Ambient temperature;
DOI:10.1021/jm00022a006

Reference yield:

: 14660-52-7
ethyl 5-bromovalerate

: 152608-82-7
3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

2: 44 percent / H₂O / 24 h / Ambient temperature

3: pivalic acid / toluene / 16 h / Heating

4: aq. HCl / tetrahydrofuran / 1 h / Ambient temperature

With hydrogenchloride; potassium carbonate; Trimethylacetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00022a006

Reference yield:

: 42216-96-6
triethyl orthoacrylate

: 152608-82-7
3-<6-<<4-<(dimethylamino)carbonyl>butyl>oxy>-2-hydroxyphenyl>propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pivalic acid / toluene / 16 h / Heating

2: aq. HCl / tetrahydrofuran / 1 h / Ambient temperature

With hydrogenchloride; Trimethylacetic acid; In tetrahydrofuran; toluene;
DOI:10.1021/jm00022a006