N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine
CAS No.:1043869-12-0
Molecular Formula:C₂₃H₃₀INO₅
Molecular Weight:527.399
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

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Chemical Property of N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

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Technology Process of N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

There total 1 articles about N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1043869-10-8
N-(tert-butoxycarbonyl)-N-(2-hydroxybenzyl)-2-(4-iodo-2-hydroxy-5-methoxyphenyl)ethylamine

: 74-88-4
methyl iodide

: 1043869-16-4
C₂₂H₂₈INO₅

: 1043869-14-2
C₂₂H₂₈INO₅

: 1043869-12-0
N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2008.04.050

Reference yield: 25.0%

: 1043869-12-0
N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

: 73183-34-3
bis(pinacol)diborane

: tert-butyl (2,5-dimethoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethyl)(2-methoxybenzyl)carbamate

Guidance literature:: With potassium acetate; In N,N-dimethyl-formamide; at 125 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201601448

Reference yield: 15.0%

: 58093-05-3
6,10-dioxaspiro<4.5>decane-7,9-dione

: 1043869-12-0
N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine

: isopropyl (4-((7,9-dioxo-6,10-dioxaspiro[4.5]decan-8-ylidene)iodanyl)-2,5-dimethoxyphenethyl)(2-methoxybenzyl)carbamate

Guidance literature:: N-(tert-butoxycarbonyl)-N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-iodophenyl)ethylamine; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

6,10-dioxaspiro<4.5>decane-7,9-dione; With sodium carbonate; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.201601448