6-nitro-2-phenylquinazoline

Base Information

• Chemical Name: 6-nitro-2-phenylquinazoline
• CAS No.: 863771-06-6
• Molecular Formula: C₁₄H₉N₃O₂
• Molecular Weight: 251.244

Synonyms:6-nitro-2-phenylquinazoline

Chemical Property of 6-nitro-2-phenylquinazoline

Chemical Property:

• Melting Point: 217-219 °C
• Boiling Point: 357.4±24.0 °C(Predicted)
• Density: 1.342±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 6-nitro-2-phenylquinazoline

There total 5 articles about 6-nitro-2-phenylquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-amino-5-nitrobenzaldehyde (56008-61-8) + benzylamine (100-46-9) → 6-nitro-2-phenylquinazoline (863771-06-6)

Guidance literature:

With TEMPOL; oxygen; In o-xylene; at 120 ℃; for 12h; under 760.051 Torr; Inert atmosphere;

DOI:10.1039/c1cc12308d

Reference yield: 61.0%

tribromomethylbenzene (2489-03-4) + 2-amino-3-(aminomethyl)benzonitrile (52098-88-1) → 6-nitro-2-phenylquinazoline (863771-06-6)

Guidance literature:

With oxygen; sodium hydroxide; In water; at 100 ℃; Sealed tube; Green chemistry;

DOI:10.1021/acs.joc.8b00327

Reference yield: 34.0%

2-phenyl-6-nitro-3,4-dihydroquinazoline (863771-07-7) → 6-nitro-2-phenylquinazoline (863771-06-6)

Guidance literature:

With chloranil; In toluene; for 1h; Heating / reflux;

upstream raw materials:

2-phenyl-6-nitro-3,4-dihydroquinazoline

2-amino-5-nitrobenzaldehyde

benzylamine

tribromomethylbenzene

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