N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

Base Information

Chemical Name:N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide
CAS No.:1343480-60-3
Molecular Formula:C₂₂H₂₄N₂O₃S
Molecular Weight:396.51
Hs Code.:

Synonyms:N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

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Technology Process of N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

There total 1 articles about N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1243147-88-7
N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamide

: 106-96-7
propargyl bromide

: 1343480-60-3
N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.08.033

Reference yield: 80.0%

: 636-98-6
p-nitrobenzene iodide

: 1343480-60-3
N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

: 1343480-67-0
N-(2,2,4-trimethyl-1-(3-(4-nitrophenyl)prop-2-ynyl)-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamide

Guidance literature:: With copper(l) iodide; palladium diacetate; triethylamine; In tetrahydrofuran; at 50 - 55 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.08.033

Reference yield: 77.0%

: 591-50-4
iodobenzene

: 1343480-60-3
N-(2,2,4-trimethyl-7-phenoxy-1-(prop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulphonamide

: 1343480-72-7
N-(2,2,4-trimethyl-7-phenoxy-1-(3-phenylprop-2-ynyl)-1,2-dihydroquinolin-6-yl)methanesulfonamide

Guidance literature:: With copper(l) iodide; palladium diacetate; triethylamine; In tetrahydrofuran; at 50 - 55 ℃; for 22h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.08.033