[(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

Base Information

Chemical Name:[(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol
CAS No.:673456-36-5
Molecular Formula:C₂₄H₃₅N₅O₅Si
Molecular Weight:501.658
Hs Code.:

Synonyms:[(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

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Chemical Property of [(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

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Technology Process of [(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

There total 3 articles about [(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 673456-35-4
C₃₈H₄₃N₅O₇Si

: 673456-36-5
[(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

Guidance literature:: With ammonia; In methanol;
DOI:10.1081/NCN-120022826

Reference yield:

: 341536-45-6
9-[2-O-acetyl-5-O-benzoyl-4-C-[(benzoyloxy)methyl]-3-O-benzyl-α-L-threo-pentofuranosyl]-6-N-benzoyladenine

: 673456-36-5
[(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NH₃ / methanol

2: 72 percent / imidazole / dimethylformamide

3: 94 percent / NH₃ / methanol

With 1H-imidazole; ammonia; In methanol; N,N-dimethyl-formamide;
DOI:10.1081/NCN-120022826

Reference yield:

: 673456-34-3
C₃₉H₃₃N₅O₈

: 673456-36-5
[(3R,4R,5R)-5-(6-Amino-purin-9-yl)-3-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxymethyl-tetrahydro-furan-2-yl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / imidazole / dimethylformamide

2: 94 percent / NH₃ / methanol

With 1H-imidazole; ammonia; In methanol; N,N-dimethyl-formamide;
DOI:10.1081/NCN-120022826