1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Base Information

Chemical Name:1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen
CAS No.:75348-18-4
Molecular Formula:C₃₂H₃₄O₇
Molecular Weight:530.618
Hs Code.:

Synonyms:1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

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Chemical Property of 1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

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Technology Process of 1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

There total 13 articles about 1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75251-60-4,75419-03-3
1L-1,7-Anhydro-1-C-hydroxymethyl-3,4:5,6-di-O-isopropyliden-2-O-methyl-chiro-inosit

: 75348-18-4
1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 9 steps

1: 89 percent / H₂O, alkaline

2: BBr₃

4: H₂O

5: 75 percent

6: H₂O, acid

7: 82 percent

9: 1) NaI, 2) POCl₃

With Alkaline; water; boron tribromide; sodium iodide; trichlorophosphate;

Reference yield:

: 100-39-0
benzyl bromide

: 75348-18-4
1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NaH / dimethylformamide / 20 h / Ambient temperature

With sodium hydride; In N,N-dimethyl-formamide;

Reference yield:

: 80971-13-7
1L-1,7-Anhydro-1-C-hydroxymethyl-5,6-O-isopropyliden-2-O-methyl-chiro-inosit

: 75348-18-4
1L-(1,3/2,4)-Di-O-acetyl-2,3,4-tri-O-benzyl-5-C-hydroxymethyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NaH / dimethylformamide / 20 h / Ambient temperature

With sodium hydride; In N,N-dimethyl-formamide;