N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

Base Information

Chemical Name:N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine
CAS No.:120703-84-6
Molecular Formula:C₂₈H₂₆ClNO₉S
Molecular Weight:588.035
Hs Code.:

Synonyms:N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

Chemical Property:

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Technology Process of N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

There total 3 articles about N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 124-63-0
methanesulfonyl chloride

: 120703-81-3
N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-β-D-ribopyranosylamine

: 120703-84-6
N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

Guidance literature:: In pyridine; at 0 ℃;
DOI:10.1016/0008-6215(88)80027-2

Reference yield:

: 98-88-4
benzoyl chloride

: 120703-84-6
N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 15 percent / pyridine / 1.) 1 h, 0 degC; 2.) 20 h, 20 degC

2: 75 percent / pyridine / 0 °C

In pyridine;
DOI:10.1016/0008-6215(88)80027-2

Reference yield:

: 56908-23-7
N-acetyl-N-p-chlorophenyl-β-D-ribopyranosylamine

: 120703-84-6
N-acetyl-3,4-di-O-benzoyl-N-p-chlorophenyl-2-O-methanesulphonyl-β-D-ribopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 15 percent / pyridine / 1.) 1 h, 0 degC; 2.) 20 h, 20 degC

2: 75 percent / pyridine / 0 °C

In pyridine;
DOI:10.1016/0008-6215(88)80027-2