1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

Base Information

Chemical Name:1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester
CAS No.:145122-58-3
Molecular Formula:C₁₆H₁₆N₂O₆
Molecular Weight:332.313
Hs Code.:

Synonyms:1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

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Chemical Property of 1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

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Technology Process of 1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

There total 2 articles about 1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.2%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 84677-06-5
(benzyloxycarbonylamino)cyclopropanecarboxylic acid

: 145122-58-3
1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; for 18h; Ambient temperature;
DOI:10.1139/v92-171

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 145122-58-3
1-Benzyloxycarbonylamino-cyclopropanecarboxylic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / NaHCO₃ / tetrahydrofuran; H₂O / 16 h / Ambient temperature

2: 79.2 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 18 h / Ambient temperature

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; water;
DOI:10.1139/v92-171