3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate

Base Information

• Chemical Name: 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate
• CAS No.: 1119193-21-3
• Molecular Formula: C₁₆H₁₇N₄*F₆P
• Molecular Weight: 410.302
• Mol file: 1119193-21-3.mol

Synonyms:3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate

Chemical Property of 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate

There total 3 articles about 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-(2-pyrimidyl)-3-(2,4,6-trimethylphenyl)-imidazolium chloride (1075753-87-5) → 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate (1119193-21-3)

Guidance literature:

With potassium hexafluorophosphate; In water; at 20 ℃; for 24h;

DOI:10.1039/C8DT03373K

Reference yield: 84.0%

2-chloropyrimidine (1722-12-9,1195939-87-7) + N-(2,4,6-trimethylphenyl)imidazole (25364-44-7) → 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate (1119193-21-3)

Guidance literature:

2-chloropyrimidine; N-(2,4,6-trimethylphenyl)imidazole; In acetonitrile; Reflux;

With ammonium hexafluorophosphate; In water;

DOI:10.1039/c7nj04836j

Reference yield:

N-(2,4,6-trimethylphenyl)imidazole (25364-44-7) → 3-(2,4,6-trimethylphenyl)-1-(pyrimidin-2-yl)-1H-imidazol-3-ium hexafluorophosphate (1119193-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 140 °C

2: potassium hexafluorophosphate / water

With potassium hexafluorophosphate; In water;

DOI:10.1021/ic403138a

upstream raw materials:

1-(2-pyrimidyl)-3-(2,4,6-trimethylphenyl)-imidazolium chloride

N-(2,4,6-trimethylphenyl)imidazole

2-chloropyrimidine