Technology Process of 4,4'-(butane-1,4-diyl)bisphenol
There total 11 articles about 4,4'-(butane-1,4-diyl)bisphenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
for 5h;
Heating;
- Guidance literature:
-
3-methoxy-1-iodobenzene; 4-ethynylphenol;
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N,N-diethylnmethylamine;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 0.333333h;
Microwave irradiation;
Inert atmosphere;
With
platinum on carbon; hydrogen;
for 12h;
Overall yield = 99%; Overall yield = 142 mg;
DOI:10.1515/znb-2015-0047
- Guidance literature:
-
4-ethynylphenol; 3-Iodophenol;
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N,N-diethylnmethylamine;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 0.333333h;
Microwave irradiation;
Inert atmosphere;
With
platinum on carbon; hydrogen;
for 12h;
Overall yield = 16%; Overall yield = 200 mg;
DOI:10.1515/znb-2015-0047
