nitrodeoxyhexestrol p-nitrobenzenesulfonate

Base Information

Chemical Name:nitrodeoxyhexestrol p-nitrobenzenesulfonate
CAS No.:76412-16-3
Molecular Formula:C₂₄H₂₄N₂O₇S
Molecular Weight:484.53
Hs Code.:

Synonyms:nitrodeoxyhexestrol p-nitrobenzenesulfonate

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Chemical Property of nitrodeoxyhexestrol p-nitrobenzenesulfonate

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Technology Process of nitrodeoxyhexestrol p-nitrobenzenesulfonate

There total 4 articles about nitrodeoxyhexestrol p-nitrobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 76412-15-2
4-Nitro-benzenesulfonic acid 4-((1R,2S)-1-ethyl-2-phenyl-butyl)-phenyl ester

: 76412-16-3
nitrodeoxyhexestrol p-nitrobenzenesulfonate

Guidance literature:: With acetic anhydride; copper(II) nitrate; at 80 ℃; for 24h;
DOI:10.1021/jm00136a013

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 76412-16-3
nitrodeoxyhexestrol p-nitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃, 2.) H₂ / 2.) 5percent Pd/C / 1.) acetone, reflux, 17 h, 2.) ethanol, 37 psi, 35 deg C

2: 97 percent / pyridine / 12 h / 70 °C

3: 81 percent / cupric nitrate trihydrate, acetic anhydride / 24 h / 80 °C

With pyridine; hydrogen; acetic anhydride; potassium carbonate; copper(II) nitrate; palladium on activated charcoal;
DOI:10.1021/jm00136a013

Reference yield:

: 3929-22-4,5776-73-8,5776-74-9
deoxyhexestrol

: 76412-16-3
nitrodeoxyhexestrol p-nitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / pyridine / 12 h / 70 °C

2: 81 percent / cupric nitrate trihydrate, acetic anhydride / 24 h / 80 °C

With pyridine; acetic anhydride; copper(II) nitrate;
DOI:10.1021/jm00136a013