4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

Base Information

Chemical Name:4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide
CAS No.:1312698-80-8
Molecular Formula:C₁₅H₁₃N₅OS₂
Molecular Weight:343.433
Hs Code.:

Synonyms:4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

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Chemical Property of 4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

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Technology Process of 4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

There total 4 articles about 4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-63-0
phenylhydrazine

: 5-(4-isothiocyanatophenyl)-1,3,4-oxadiazole-2-thiol

: 1312698-80-8
4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

Guidance literature:: In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1312698-80-8
4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / 1 h / Reflux

2.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

2.2: pH 4

3.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

4.1: toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 5351-17-7
4-aminobenzohydrazide

: 1312698-80-8
4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

1.2: pH 4

2.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

3.1: toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017