4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

Base Information

Chemical Name:4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate
CAS No.:1581275-72-0
Molecular Formula:C₃₁H₂₇N₃O₄S
Molecular Weight:537.639
Hs Code.:

Synonyms:4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

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Chemical Property of 4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

Chemical Property:

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Technology Process of 4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

There total 5 articles about 4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 1581275-72-0
4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium acetate / ethanol / 0.5 h / 20 °C

2: N,N-dimethyl-formamide / 12 h / 20 °C / Irradiation

3: thionyl chloride / 2 h / Reflux

4: triethylamine / tetrahydrofuran / 20 °C

With thionyl chloride; ammonium acetate; triethylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm401721h

Reference yield:

: 80459-48-9
4-tosyloxybenzaldehyde

: 1581275-72-0
4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: water; sodium tetrahydroborate / 0 °C / Inert atmosphere

3: triethylamine / tetrahydrofuran / 20 °C

With sodium tetrahydroborate; water; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1021/jm401721h

Reference yield:

: 89242-54-6
4-phenylquinazoline-2-carboxylic acid

: 1581275-72-0
4-((N-ethyl-4-phenylquinazoline-2-carboxamido)methyl)-phenyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Reflux

2: triethylamine / tetrahydrofuran / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm401721h