N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

Base Information

Chemical Name:N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine
CAS No.:1350430-04-4
Molecular Formula:C₁₄H₂₁Br₃N₂O
Molecular Weight:473.046
Hs Code.:

N<SUP>1</SUP>,N<SUP>1</SUP>-dimethyl-N<SUP>3</SUP>-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

Synonyms:N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

Chemical Property:

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Technology Process of N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

There total 6 articles about N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1359715-08-4
2-(2,4,6-tribromo-3-methoxyphenyl)acetaldehyde

: 109-55-7
1-amino-3-(dimethylamino)propane

: 1350430-04-4
N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

Guidance literature:: 2-(2,4,6-tribromo-3-methoxyphenyl)acetaldehyde; 1-amino-3-(dimethylamino)propane; In methanol; at 65 ℃; Microwave irradiation; Sealed tube;

With sodium tetrahydroborate; In methanol; at 100 ℃; Microwave irradiation; Sealed tube;
DOI:10.1016/j.ejmech.2013.12.050

Reference yield:

: 1359715-06-2
2-(2,4,6-tribromo-3-methoxyphenyl)ethanamine

: 109-54-6
3-(Dimethylamino)propyl chloride

: 1350430-04-4
N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

Guidance literature:: With sodium hydroxide; In chloroform; water; at 140 ℃; for 0.166667h; pH=10; Microwave irradiation;
DOI:10.1016/j.ejmech.2013.12.050

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 1350430-04-4
N¹,N¹-dimethyl-N³-(2,4,6-tribromo-3-methoxyphenethyl)propane-1,3-diamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine; acetic acid / water / 5 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3.1: sodium ethanolate / toluene

3.2: Reflux

4.1: clay K₁₀ / methanol / 65 °C / Microwave irradiation; Sealed tube

4.2: 100 °C / Microwave irradiation; Sealed tube

With bromine; sodium ethanolate; potassium carbonate; acetic acid; In methanol; water; N,N-dimethyl-formamide; toluene; 3.1: |Darzens Condensation;
DOI:10.1016/j.ejmech.2013.12.050