2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

Base Information

Chemical Name:2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester
CAS No.:797800-63-6
Molecular Formula:C₁₈H₂₂Cl₃NO₆
Molecular Weight:454.735
Hs Code.:

Synonyms:2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

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Chemical Property of 2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

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Technology Process of 2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

There total 1 articles about 2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 4124-31-6
trichloroacetic acid anhydride

: 2-isocyano-2-(4-methoxy-benzyl)-pent-4-enoic acid ethyl ester

: 797800-63-6
2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

Guidance literature:: trichloroacetic acid anhydride; 2-isocyano-2-(4-methoxy-benzyl)-pent-4-enoic acid ethyl ester; In dichloromethane; at -20 - 20 ℃;

With water; In dichloromethane; Further stages.;
DOI:10.1016/j.tetlet.2004.08.169

Reference yield: 72.0%

: 459-73-4
GlyOEt*HCl

: 797800-63-6
2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

: 2-[(ethoxycarbonylmethyl-aminooxalyl)-amino]-2-(4-methoxy-benzyl)-pent-4-enoic acid ethyl ester

Guidance literature:: 2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester; With chloro-trimethyl-silane; triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

GlyOEt*HCl; In tetrahydrofuran; at 20 ℃; for 72h; Further stages.;
DOI:10.1016/j.tetlet.2004.08.169

Reference yield: 68.0%

: 123-75-1
pyrrolidine

: 797800-63-6
2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester

: 2-(4-methoxy-benzyl)-2-(2-oxo-2-pyrrolidin-1-yl-acetylamino)-pent-4-enoic acid ethyl ester

Guidance literature:: 2-(4-methoxy-benzyl)-2-(3,3,3-trichloro-2,2-dihydroxy-propionylamino)-pent-4-enoic acid ethyl ester; With chloro-trimethyl-silane; triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

pyrrolidine; In tetrahydrofuran; at 20 ℃; for 15h; Further stages.;
DOI:10.1016/j.tetlet.2004.08.169